多接收等离子质谱实验室

MC-ICP-MS实验室成立于2015年,主要利用电感耦合等离子体质谱(MC-ICP-MS)与各类溶液进样设备(如膜去溶,氢化物发生器等)联用,开展地质样品的同位素分析。针对地学领域的科学问题,研发了一系列Li-Fe-Ge-Ag-Hg稳定同位素以及Sr-Nd-Pb-Hf放射性同位素等分析方法,并将这些方法广泛应用于成矿过程研究、古环境示踪、壳-幔物质循环等诸多研究领域。

实验室始终保持对外开放与合作的工作模式,吸引了大量国内外同行来实验室开展分析与合作研究。自实验室成立以来,先后有来自中国科学院(如中科院广州地化所、中科院地理所)和国内高校(如中国地质大学、厦门大学、中山大学、中国科学技术大学、北京大学、成都理工大学、长安大学)以及美国、韩国、香港等单位和地区的科学家来实验室进行合作研究,并取得了大量成果。


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    仪器名称:多接收电感耦合等离子质谱仪(Neptune plus)

    启用时间:2014年9月

    主要技术指标:

    分析元素范围:Li―U;高分辨率≥8000;

    普通灵敏度:U≥40V/ppm;

    高灵敏度:U≥1200V/ppm;

    内精度:87Sr/86Sr、143Nd/144Nd、207Pb/206Pb、176Hf/177Hf均优于20ppm;206Pb/204Pb、235U/238U均优于200 ppm;

    丰度灵敏度(237U):<0.5ppm;

    噪音(Dark noise):离子计数器< 0.1 cps;法拉第杯40μV (1 s积分时间)。

    主要功能及应用:

    适用于矿物、岩石、水样以及陨石样品的同位素比值测定,包括放射性同位素体系和稳定同位素体系,是研究宇宙起源、成矿物质来源、地表风化过程、古环境的等地质过程的重要手段。


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      实验室人员


      周汀,工程师

      主要从事同位素地球化学研究。负责MC-ICP-MS实验室的日常操作,维护以及同位素测试方法的开发,在国内外主流刊物如EPSL,JAAS上发表SCI论文5篇。

      Email:zhouting@mail.gyig.ac.cn

      电话:0851-8439 4737

      办公地点:A3楼323房间/110房间





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        内容筹备中


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          方法文章示例:

          Ge同位素:Zhou, T., L. Qi, and J. Xu (2025), An Improved Hydride Generation System for Isotope Measurement usink, g Multi-collector ICP-MS: A Case Study of Germanium Isotopes, At. Spectrosc.

          低含量Nd-Hf同位素:Zhou, T., L. Qi, S.-h. Liu, and B. Zhou (2024), A simplified instrumental protocol for trace Nd and Hf isotope measurements (< 10 ng) using a MC-ICP-MS and an Apex Omega de-solvating system, J. Anal. At. Spectrom., doi:DOI https://doi.org/10.1039/D4JA00276H.

          Ag同位素:Gong, H., Y. Qi, T. Lan, H. Fan, Y. Chen, T. Zhou, and R. Hu (2024), Accurate determination of stable silver isotopes in zinc-rich samples through effective separation of silver and zinc, J. Anal. At. Spectrom., 39(8), 1980-1989.

          Li同位素:Xu, L., C. Luo, and H. Wen (2020b), A revisited purification of li for ‘Na breakthrough’and its isotopic determination by MC‐ICP‐MS, Geostandards and Geoanalytical Research, 44(1), 201-214.

          Sr同位素:Zhou, T., L. Qi, H. Fan, and R. Yin (2020), An optimized protocol for high precision measurement of 87 Sr/86 Sr using a Neptune Plus multi-collector inductively coupled plasma mass spectrometer: evaluation of different cone combinations for Sr isotope determination, Analytical Methods, 12(32), 4089-4096, doi:DOI https://doi.org/10.1039/D0AY00845A.

          Mo同位素:Liu, J., H. Wen, Y. Zhang, H. Fan, and C. Zhu (2016), Precise Mo isotope ratio measurements of low-Mo (ng g− 1) geological samples using MC-ICP-MS, J. Anal. At. Spectrom., 31(6), 1287-1297.

          Zn同位素:Yang, Y., X. Zhang, S.-A. Liu, T. Zhou, H. Fan, H. Yu, W. Cheng, and F. Huang (2018), Calibrating NIST SRM 683 as a new international reference standard for Zn isotopes, J. Anal. At. Spectrom., 33(10), 1777-1783.

          地质应用文章示例:

          低含量Nd-Hf应用:

          Chen, J.-F., Y.-Y. S. Zhao, Q. Shu, S.-H. Zhou, W. Du, and J. Yang (2024), The oxygen fugacity of intermediate shergottite NWA 11043: implications for Martian mantle evolution, Geochim. Cosmochim. Acta, 375, 90-105.

          Huang, F., J. Li, J. Xu, J. Chen, B. Wang, P. Hu, R. Xu, Y. Zeng, L. Zhang, and T. Zhou (2023), Mo isotopes archive oceanic sediments in post-orogenic lithospheric mantle, Geochim. Cosmochim. Acta, 341, 75-89.

          Zhou, S.-H., Q. Shu, D. G. Pearson, D. Li, Y. Xu, and J. Liu (2023), Rejuvenation of the lithospheric mantle beneath the orogens: Constraints from elemental geochemistry and Os isotopes in mantle xenoliths, Geochim. Cosmochim. Acta, 349, 96-114.

          Zn同位素应用:

          Fan, H., H. Wen, C. Xiao, T. Zhou, C. Cloquet, and X. Zhu (2018), Zinc Geochemical Cycling in a Phosphorus‐Rich Ocean During the Early Ediacaran, Journal of Geophysical Research: Oceans, 123(8), 5248-5260.

          Xu, C., H. Zhong, R.-Z. Hu, H.-J. Wen, W.-G. Zhu, Z.-J. Bai, H.-F. Fan, F.-F. Li, and T. Zhou (2020a), Sources and ore-forming fluid pathways of carbonate-hosted Pb–Zn deposits in Southwest China: implications of Pb–Zn–S–Cd isotopic compositions, MinDe, 55(3), 491-513.

          Ge同位素应用:Qi, H.-W., R.-Z. Hu, K. Jiang, T. Zhou, Y.-F. Liu, and Y.-W. Xiong (2019), Germanium isotopes and Ge/Si fractionation under extreme tropical weathering of basalts from the Hainan Island, South China, Geochim. Cosmochim. Acta, 253, 249-266, doi:https://doi.org/10.1016/j.gca.2019.03.022.

          Ga同位素应用:

          Zhang, Y., S. Liao, C. Tao, H. Wen, H. Fan, J. Wen, W. Yang, and W. Li (2021), Ga isotopic fractionation in sulfides from the Yuhuang and Duanqiao hydrothermal fields on the Southwest Indian Ridge, Geoscience Frontiers, 12(4), 101137-101137.

          Cd同位素应用:

          Zhang, Y., H. Wen, C. Zhu, H. Fan, and C. Cloquet (2018), Cadmium isotopic evidence for the evolution of marine primary productivity and the biological extinction event during the Permian-Triassic crisis from the Meishan section, South China, Chem. Geol., 481, 110-118.

          Hg同位素应用:

          Zhou, T., X. Pan, R. Sun, C. Deng, J. Shen, S. Y. Kwon, S. E. Grasby, J. Xiao, and R. Yin (2021), Cryogenian interglacial greenhouse driven by enhanced volcanism: Evidence from mercury records, Earth. Planet. Sci. Lett., 564, 116902, doi:10.1016/j.epsl.2021.116902.

          Li同位素应用:

          Hu, N., R. Hu, H. Chen, S. Fu, J. Yang, L. Xu, and C. Luo (2024), Lithium and oxygen isotopic constraints on the source and evolution of ore-forming fluids: a case study from the Shuiyindong Carlin-type gold deposit, SW China, MinDe, 59(2), 313-328.



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