The AMS Laboratory

Introduction to the AMS Laboratory

  Long-lived radioactive nuclides (such as 10Be, 14C, 26Al, 41Ca, and 129I, etc.) generated by nuclear reactions between cosmic rays and the Earth's atmosphere (atmospheric origin), rocks on the Earth's surface (in situ origin), or extraterrestrial substances have been used in various fields including environmental tracing, geochronology, hydrology, archaeology, and planetary science. To meet the demands of material cycle in karst areas and to enhance applications in planetary science, IGCAS purchased a state of art accelerator mass spectrometer (AMS) from NEC Company USA in 2017.This AMS laboratory represents the first AMS facility established in southwestern China and is dedicated to conducting research on 14C, 10Be, and 26Al chronology and environmental tracing among other applications.


The current testing projects:

Measurement of 14C:

Tracing of inorganic carbon (DIC) and organic carbon (DOC, POC) in water samples.

14C chronology and source tracing of soil/deposit.

14C environmental tracing of atmosphere (aerosols, CO2).

14C archaeology (bone collagen, silk fabrics, etc.).

Tracing of organic carbon sources of biomass (algae, zooplankton, plants, seeds, etc.).

14C of solid inorganic carbon (corals, shells, foraminifera, stalagmites, carbonate rocks)

Measurement of 10Be and 26Al

In-situ 10Be/26Al in quartz. 

10Be in marine sediments. 

10Be in soil and atmosphere. 

10Be/26Al in extraterrestrial samples.


附件:

    The main equipment in the laboratory is a 1MV multi-isotope AMS, which was imported from the US NEC company (model: 3SDH-1 UAMS). Recently, it has mainly been used for the analysis of 10Be, 14C and 26Al. In the future, the measurement methods for 41Ca and 129I will be developed. Based on the acceptance results and the test results of over 500 samples completed so far, the measurement accuracy of 14C is better than0.3%(OXII standard) and the instrument background can reach 3×10-16(Alpha Graphite). The abundance sensitivity of 10Be and 26Al can reach 5×10-15, and the measurement accuracy is better than 1% (10-11 level standard).

    To avoid the interference of environmental primordial nuclides on 10Be and 26Al in ultra-trace geological age samples, an ultra-clean chemical laboratory for the chemical treatment of 10Be and 26Al samples has been established. The laboratory is equipped with dedicated fume hoods, muffle furnaces, ovens, etc.

    A systematic 14C sample (gas-solid-liquid-biological) pre-treatment and sample preparation laboratory has been established, with 2 sets of manual vacuum lines and 1 set of automatic graphitization system (Aeon CEGS 12X), which can be used for the preparation of carbon samples as low as 100 μg.

    1MV AMS

    10Be测量二维能谱

    10Be测量稳定性

    10Be26Al超净实验室

    14C测量稳定性 

    14C前处理系统

    26Al测量稳定性



    附件:

      Scientific researcher

      Dr. Liu Yu, Associate Professor.

      Her research interests focus on the cosmogenic nuclides and their application in geomorphology and geochronology. Currently, she holds the position of head of the 1.0 MV AMS Laboratory within the Environmental Department. Her primary responsibilities include laboratory management, as well as the development and implementation of sample pre-treatment technologies for 10Be and 26Al.

      Laboratory: Room 202, 203, Building 5

      Office: Room 301, Building 2

      Email: liuyu@mail.gyig.ac.cn

      Personal access link: https://skleg.gyig.ac.cn/kydw/fyjy/202408/t20240816_239174.html

      Technicians in AMS Laboratory

      Dr. Yang Haiquan, Senior Engineer.

      His primary responsibility is to conduct development of 14C pre-treatment methods and explore their applications.

      Responsible instrument: Aeon CEGS 12X

      Laboratories: Room 207, Building 2; Room 207, 208, Building 5

      Office: Room 508, Building 2

      Email: yanghaiquan@vip.skleg.cn

      Dr. Yang Xianlin, engineer. 

      His primary responsibilities include the operation and maintenance of AMS as well as the development of analytical methodologies. Currently, he is engaged in research on high-energy proton and neutron nuclear data measurement utilizing AMS technology.

      Responsible instrument: 3SDH-1 UAMS

      Laboratory: Room 104 and 105 of Building 5

      Office: Room 204 of Building 5

      Email: yangxianlin@mail.gyig.ac.cn


      附件:

        Laboratory reservation process and charging standards

        You can contact the heads of each laboratory via email. The detailed fee standards are as shown in the table below.

        Items

        Charging standards

        Notes

        The processed AMS sample target

        14C

        ¥1200 yuan

        1. If the sample you have prepared requires the target pressing service, you will need to pay an additional fee. The charge for10Be is 200 yuan per sample, for26Al is 150 yuan per sample, and for14C is 100 yuan per sample.

        2. If the user agrees to share the results (co-authoring the publication), and after approval by the leader, a discounted price can be offered.

        10Be

        ¥1200 yuan

        26Al

        ¥1200 yuan

        14C-pretreatment

        No chemical process samples

        ¥1800 yuan

        with chemical process sample

        ¥2300 yuan

        10Be and26Al pretreatment

        Rock samples with single nuclides of10Be or26Al

        ¥6000 yuan

        Sand samples with a single nuclide of10Be or26Al

        ¥5800 yuan

        Rock samples with dual nuclides of10Be and26Al

        ¥7500 yuan

        Sand samples with10Be and26Al dual nuclides

        ¥7300 yuan

        Soil sample (only10Be)

        ¥5000 yuan

        Marine sediments (only10Be)

        ¥5000 yuan


        附件:

          User notes

          The testing accuracy of the instruments and the background are closely related to the sample type, chemical pretreatment, instrument stability, data processing, etc. Currently, the testing accuracy provided by the instruments is the standard testing accuracy for each nuclide, not the actual sample testing accuracy. Therefore, the sample submitter needs to inform the instrument staff of the key information of the sample to be tested (such as carbon content) in advance.

          This laboratory only conducts measurements on naturally low-radioactive samples. It does not measure biological samples with artificially added tracers, samples related to nuclear activities, nuclear facilities, uranium mines, etc. with high radioactivity. Please inform the sample submitter of the sample source in advance and make a commitment. If there is any false information or concealment, this laboratory has the right to hold the submitter legally responsible. 

          This laboratory is mainly used for basic scientific research. It does not bear legal responsibility for samples involving commercial value disputes.

          Before entering this laboratory to conduct experiments, users are kindly requested to read relevant precautions and literature in advance to understand sample preparation and technical methods, etc.

          References

          1. The 10Be/26Al in In-situ quartz

          Liu, Y., Xu, S., Fabel, D., Rode, A., Zhang, X.B., et al., 2025. Cosmogenic 10Be and 26Al dating of the fluvial terraces in the Sichuan Basin, SW China: Implications for the drainage evolution of the middle Yangtze River. Quaternary Science Reviews, 369: 109653.

          Liu, Y., Sun, L., Xu, S., Ma, Y., et al., 2023. Cosmogenic nuclide chronological constraints on the late Cenozoic strata of the Linxia Basin, northeast Tibetan Plateau. Palaeogeography, Palaeoclimatology, Palaeoecology, 626: 111695.

          Liu, Y., Liu, X.B., Wang, S.J., Xu, S., et al., 2022. Late Cenozoic channel migration of the proto-Yangtze River in the delta region: Insights from cosmogenic nuclide burial dating of onshore boreholes. Geomorphology, 407: 108228.

          Liu, Y., Wang, S.J., Xu, S., Fabel, D., et al., 2022. New chronological constraints on the Plio-Pleistocene uplift of the Guizhou Plateau, SE margin of the Tibetan Plateau. Quaternary Geochronology, 67: 101237.

          2. the 10Be in ocean sediments

          Chu, Y.Z., Li, X.H., Yi, L., Dong, Y.H., Xie, R.F.C., Fan, Z.D., Hein, J.R., Little, S.H., Liu, Y., Matsuzaki, H. et al., 2025. A shift in ocean circulation drives variations in paleoproductivity in the North Pacific Ocean. Earth and Planetary Science Letters, 671: 119669.

          Konstantinova, N., Hein, J.R., Yi, L., Liu, Y., Matsuzaki, H. et al., 2025. Refined Os isotope stratigraphy of ferromanganese crusts from the Arctic Ocean and implications for polar environmental change since the late Miocene. Sedimentary Geology, 486: 106942.

          3. 14C in water

          Chao Yin, Yan Zeng, Jingan Chen, Guangrong Ran, Haiquan Yang, Jia Yu, Jingfu Wang, Ziyan Zhang, Xudong Guo. Quantitatively tracing the decomposition of endogenous particulate organic carbon during sinking in (sub-)deep reservoirs: Using radiocarbon isotopes Δ14C. Water Research. 2025. 271, 123003.

          Jingan Chen, Haiquan Yang, Yan Zeng, Jianyang Guo, Yilong Song, Wei Ding. Combined use of radiocarbon and stable carbon isotope to constrain the sources and cycling of particulate organic carbon in a large freshwater lake, China. Science of the Total Environment. 2018, 625:27-38.

          4. AMS and nuclear data

          Xian-Lin Yang, Chang-Lin Lan, Yu-Ting Wei, Yi Zhang, Gong Jiang, Bo Xie, Yu Liu, Hong-Tao Shen & Xiao-Jun Sun. Cross section determination of 27Al(n,2n)26Al reaction induced by 14-MeV neutrons uniting with D-T neutron activation and AMS techniques. NUCL SCI TECH 35, 94 (2024).


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